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247599

Antimicrobial and antioxidant evaluation of newly synthesized nanomaterials of potential anticorrosion properties based on Co (II), Ni (II), Cu (II) and Zn (II) nano complexes of

Article

Last updated: 01 Jan 2025

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Subjects

-

Tags

Organic chemistry

Abstract

Abstract

Microwave and traditional methods were used to synthesis a novel derivative of the thiourea ligand N-(p-methylphenyl)-N'-Benzoyl thiourea (MBT) and its transition metal complexes of Co (II), Ni (II), Cu (II), and Zn (II). Elemental analysis, FT-IR, mass spectroscopy, 1HNMR, 13CNMR, and UV-Visible were used to investigate the structure of MBT ligand and their complexes. Geometry of proposed chelate complexes was studied using electronic spectra, electron spin resonance (ESR), and magnetic susceptibility. Thermal gravimetric analysis (TGA) was used to study the solidity of complexes. X- ray diffraction XRD was used to investigate the surface morphologies of solid complexes. Antimicrobial activity of MBT ligand and their complexes was investigated. Also proposed chelate complexes were examined in vitro by radical scavenging activity (DPPH) to evaluate their antioxidant activity. The anticorrosion activity of the ligand was studied by weight loss method

DOI

10.21608/ejchem.2022.145699.6346

Keywords

microwave-assisted synthesis, Thiourea derivative, antibacterial and antifungal activity, DPPH radical scavenging and anticorrosion activity

Authors

First Name

KHALID

Last Name

WAHDAN

MiddleName

MARZOUK

Affiliation

Chemistry department, faculty of Science, Al Azhar university , Cairo , Egypt

Email

k_wahdan@yahoo.com

City

TANTA

Orcid

-

First Name

Eman

Last Name

Zarie

MiddleName

Said

Affiliation

Department of Therapeutic Chemistry, Institute of pharmaceutical Science and drug Industries Research , National Research Centre

Email

eman.said.zarie1@gmail.com

City

-

Orcid

0000-0002-4211-3105

First Name

Zaghloul

Last Name

Elbialy

MiddleName

Ibrahim

Affiliation

Egyptian Organization for Standardization and Quality

Email

zaghloul55@gmail.com

City

Cairo

Orcid

-

First Name

Ali

Last Name

Wahba

MiddleName

Mustafa Hassan

Affiliation

Al Azhar University

Email

alimhassanuk@yahoo.co.uk

City

Cairo

Orcid

0000-0001-9509-9266

First Name

Bassem H.

Last Name

Heakal

MiddleName

-

Affiliation

Egyptian Organization for Standardization and Quality

Email

ahmadramzy1911@gmail.com

City

cairo

Orcid

-

First Name

Ahmed

Last Name

Said

MiddleName

Osman

Affiliation

Senior researcher chemist, Greater Cairo Water Company, Cairo,

Email

chem2you@gmail.com

City

Cairo

Orcid

0000-0002-2473-9315

Volume

65

Article Issue

132

Related Issue

39238

Issue Date

2022-12-01

Receive Date

2022-06-19

Publish Date

2022-12-01

Page Start

1,253

Page End

1,268

Print ISSN

0449-2285

Online ISSN

2357-0245

Article File

EJCHEM_Volume 65_Issue 132_Pages 1253-1268.pdf

PDF . 2.1MB

Link

https://ejchem.journals.ekb.eg/article_247599.html

Detail API

https://ejchem.journals.ekb.eg/service?article_code=247599

Order

247,599

Type

Original Article

Type Code

297

Publication Type

Journal

Publication Title

Egyptian Journal of Chemistry

Publication Link

https://ejchem.journals.ekb.eg/

MainTitle

Antimicrobial and antioxidant evaluation of newly synthesized nanomaterials of potential anticorrosion properties based on Co (II), Ni (II), Cu (II) and Zn (II) nano complexes of

Details

Type

Article

Created At

30 Dec 2024