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312726

Synthesis and Antimicrobial Activity of Novel Bisbenzoxazine Monomer

Article

Last updated: 29 Dec 2024

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-

Tags

Chemistry

Abstract

In this research, a compound called 2,2'-((1E,1'E)-(hexane-1,6-diylbis(azanylylidene))bis(methanylylidene))diphenol (SA-HMDASF) was synthesized by combining salicylaldehyde and hexamethylene diamine. The resulting SA-HMDASF was then reduced using sodium borohydride, leading to the formation of 2,2'-((hexane-1,6-diylbis((SA-HMDA-NH) through a chemical reaction. Subsequently, SA-HMDA-NH was reacted with formaldehyde, resulting in the production of a benzoxazine monomer called SA-HMDA-BZ. To determine the chemical composition of SA-HMDA-BZ, different analytical methods such as FT-IR, 1H, and 13C NMR spectroscopy were employed. These methods were crucial in identifying and confirming the molecular composition and arrangement of the compound. Furthermore, Scanning Electron Microscopy (SEM) was used to analyze the surface morphology of SA-HMDA-BZ while its crystalline properties were assessed through X-ray Diffraction (XRD) analysis. These characterization techniques provided valuable insights into the physical attributes and structural properties of SA-HMDA-BZ. Additionally, the antimicrobial activity of SA-HMDA-BZ was investigated, and the results displayed promising outcomes. The compound exhibited notable antimicrobial properties, suggesting its potential as an effective agent against various microorganisms.

DOI

10.21608/sjsci.2023.218511.1088

Keywords

Benzoxazine, Crystallinity, Thermal stability and Antimicrobial activity

Authors

First Name

Ahmed

Last Name

Soliman

MiddleName

-

Affiliation

Department of Chemistry, Faculty of Science, Sohag University, Sohag 82524, Egypt.

Email

a_sol2000@yahoo.com

City

-

Orcid

-

First Name

Kamal

Last Name

Aly

MiddleName

I

Affiliation

Polymer Research Laboratory, Chemistry Department, Faculty of Science, Assiut University, Assiut 71516, Egypt.

Email

kamalaly@aun.edu.eg

City

Sohag

Orcid

-

First Name

Amer

Last Name

Amer

MiddleName

A

Affiliation

Department of Chemistry, Faculty of Science, Sohag University, Sohag 82524, Egypt.

Email

amer_chem@yahoo.com

City

Sohag

Orcid

org/0000-0001-7112-9918

First Name

Ahmed

Last Name

Abdel-Aziz

MiddleName

E

Affiliation

Department of Botany and Microbiology, Faculty of Science, New Valley University, El-Kharga 72511, Egypt.

Email

aahmedelbadry@yahoo.com

City

New Valley

Orcid

-

First Name

Mohamed

Last Name

Mohamed

MiddleName

Gamal

Affiliation

Polymer Research Laboratory, Chemistry Department, Faculty of Science, Assiut University, Assiut 71516, Egypt., Department of Materials and Optoelectronic Science, College of Semiconductor and Advanced Technology Research, Center for Functional Polymers and Supramolecular Materials, National Sun Yat-Sen University, Kaohsiung, 804, Taiwan.

Email

mgamal.eldin12@aun.edu.eg

City

Assuit

Orcid

-

First Name

Mostafa

Last Name

Belal

MiddleName

Rabie

Affiliation

Department of Chemistry, Faculty of Science, Sohag University, Sohag 82524, Egypt.

Email

mostafarabie2022@science.sohag.edu.eg

City

Sohag

Orcid

https://orcid.org/00

Volume

9

Article Issue

1

Related Issue

42891

Issue Date

2024-03-01

Receive Date

2023-06-20

Publish Date

2024-01-01

Page Start

1

Page End

6

Print ISSN

2357-0938

Online ISSN

2974-4296

Article File

SJSCI_Volume 9_Issue 1_Pages 1-6.pdf

PDF . 572.5kB

Link

https://sjsci.journals.ekb.eg/article_312726.html

Detail API

https://sjsci.journals.ekb.eg/service?article_code=312726

Order

312,726

Type

Regular Articles

Type Code

2,359

Publication Type

Journal

Publication Title

Sohag Journal of Sciences

Publication Link

https://sjsci.journals.ekb.eg/

MainTitle

Synthesis and Antimicrobial Activity of Novel Bisbenzoxazine Monomer

Details

Type

Article

Created At

29 Dec 2024