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395681

Effortless green synthesis of zero-valent copper nanoparticles

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Last updated: 29 Dec 2024

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Abstract

We present a direct, environmentally friendly approach for synthesizing porous zero-valent copper nanoparticles utilizing green tea as both a reducing and stabilizing agent. The synthesis procedure was efficient, economical, and eco-friendly. The impact of the reactants' mixing ratio was examined. Optimal yield, around 70%, was attained at 158°F with stirring for 2 hours at 1000 revolutions per minute. The resulting pellet was rinsed three times with distilled water and ethanol. The nanoparticles were dehydrated in a hot air oven at 122 °F. Nanoparticle formation was confirmed via visible color change, UV-visible spectroscopy (UV-Vis), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), zeta potential measurement, scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), and transmission electron microscopy (TEM). The XRD analysis revealed that the particles exhibited an average crystallite size of around 25 nm. SEM scans validate its oval morphology.

DOI

10.21608/jbes.2024.395681

Keywords

green tea, copper, Zero-valent, Nanoparticles

Authors

First Name

Ahmed E.

Last Name

Mostafa

MiddleName

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Affiliation

Chemistry Department, Faculty of Science, Benha University, Benha, Egypt

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First Name

Hesham H.

Last Name

El-Fey

MiddleName

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Affiliation

Chemistry Department, Faculty of Science, Benha University, Benha, Egypt

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City

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Orcid

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First Name

Mostafa Y.

Last Name

Nassar

MiddleName

-

Affiliation

Chemistry Department, Faculty of Science, Benha University, Benha, Egypt

Email

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City

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Orcid

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First Name

Hisham Marawan

Last Name

Aly

MiddleName

-

Affiliation

Chemistry Department, Faculty of Science, Benha University, Benha, Egypt

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-

City

-

Orcid

-

Volume

11

Article Issue

4

Related Issue

51467

Issue Date

2024-10-01

Receive Date

2024-12-07

Publish Date

2024-10-01

Page Start

615

Page End

625

Print ISSN

2536-9202

Online ISSN

2356-6388

Link

https://jbes.journals.ekb.eg/article_395681.html

Detail API

https://jbes.journals.ekb.eg/service?article_code=395681

Order

395,681

Type

Original Article

Type Code

3,063

Publication Type

Journal

Publication Title

Journal of Basic and Environmental Sciences

Publication Link

https://jbes.journals.ekb.eg/

MainTitle

Effortless green synthesis of zero-valent copper nanoparticles

Details

Type

Article

Created At

21 Dec 2024