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370584

Effect of Synthetic Route on the Structure and Morphology of ZnM2O4, M= (Fe, Cr, Mn, Al) Nano-oxides

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Last updated: 05 Jan 2025

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Abstract

Nano-crystalline ZnM2O4, M= (Al, Fe, Cr, Mn) particles have been prepared by different methods such as combustion,
hydrothermal and sol-gel methods. The samples were characterized by X-ray diffraction (XRD) analysis, Fourier transform
infrared spectroscopy (FTIR) and Transmission Electron Microscope (TEM). The XRD analysis showed that the samples exhibit
different crystal phases depending on the preparation route. Itshowed that pure spinel phases formed only by combustion method
with crystallite sizes lie in the range of 6 – 37 nm. The particulate and morphological properties have been investigated using
TEM techniques.

DOI

10.21608/jbes.2019.370584

Keywords

ZnCr2O4, ZnAl2O4, ZnMn2O4, XRD, Spinel

Authors

First Name

M.

Last Name

Khairy

MiddleName

-

Affiliation

Chemistry Department, Faculty of Science, Benha University, Benha, Egypt. Chemistry Department, College of Science, Al-Imam Mohammad Ibn Saud lslamic University, Riyadh, KSA

Email

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City

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Orcid

-

First Name

M.

Last Name

Sameeh

MiddleName

-

Affiliation

Chemistry Department, Faculty of Science, Benha University, Benha, Egypt

Email

-

City

-

Orcid

-

First Name

T.

Last Name

Esawy

MiddleName

-

Affiliation

Chemistry Department, Faculty of Science, Benha University, Benha, Egypt.

Email

-

City

-

Orcid

-

First Name

W. A.

Last Name

Bayoumy

MiddleName

-

Affiliation

Chemistry Department, Faculty of Science, Benha University, Benha, Egypt.

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-

City

-

Orcid

-

Volume

6

Article Issue

1

Related Issue

49537

Issue Date

2019-01-01

Receive Date

2024-07-29

Publish Date

2019-01-01

Page Start

45

Page End

52

Print ISSN

2536-9202

Online ISSN

2356-6388

Article File

JBES_Volume 6_Issue 1_Pages 45-52.pdf

PDF . 684.5kB

Link

https://jbes.journals.ekb.eg/article_370584.html

Detail API

https://jbes.journals.ekb.eg/service?article_code=370584

Order

370,584

Type

Original Article

Type Code

3,063

Publication Type

Journal

Publication Title

Journal of Basic and Environmental Sciences

Publication Link

https://jbes.journals.ekb.eg/

MainTitle

Effect of Synthetic Route on the Structure and Morphology of ZnM2O4, M= (Fe, Cr, Mn, Al) Nano-oxides

Details

Type

Article

Created At

21 Dec 2024