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221404

Synthesis of mesoporous -Ga2O3 nanorods by sol-gel method in aqueous medium using -irradiated gallium chloride precursor

Article

Last updated: 05 Jan 2025

Subjects

-

Tags

Chemistry

Abstract

Mesoporous structures -Ga2O3 nanorods have been synthesized by sol-gel method using gelatin, water and -Irradiated gallium chloride with 102 kGy total -ray absorbed dose as starting materials. The transparent gel containing gallium ions was calcined at 600 C for 4 hours to form -Ga2O3 nanorods. The as- synthesized -Ga2O3 nanorods were characterized by x-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM) and Fourier – transform infrared spectroscopy (FT-IR). From x-ray diffraction patterns, the purity and crystallinity nature of the as-synthesized nanoparticles were tested. Based on the infrared spectra of the as-synthesized nanoparticles, the IR bands attributed to GaO and lattice vibration of -Ga2O3 were recorded in the wavenumber range of (400- 4400 cm-1). TEM image of the as-synthesized nanoproducts displays the formation of -Ga2O3 nanorods. The role of -Irradiation on the synthesis of -Ga2O3 nanorods was evaluated and discussed.

DOI

10.21608/aunj.2017.221404

Keywords

Mesoporous structure, Ga2O3 nanorods, Gamma Irradiation

Volume

46

Article Issue

1

Related Issue

31576

Issue Date

2017-06-01

Receive Date

2022-02-23

Publish Date

2017-06-01

Page Start

26

Page End

30

Print ISSN

2812-5029

Online ISSN

2812-5037

Link

https://aunj.journals.ekb.eg/article_221404.html

Detail API

https://aunj.journals.ekb.eg/service?article_code=221404

Order

221,404

Type

Novel Research Articles

Type Code

2,242

Publication Type

Journal

Publication Title

Assiut University Journal of Multidisciplinary Scientific Research

Publication Link

https://aunj.journals.ekb.eg/

MainTitle

Synthesis of mesoporous -Ga2O3 nanorods by sol-gel method in aqueous medium using -irradiated gallium chloride precursor

Details

Type

Article

Created At

23 Jan 2023