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147994

Controlling the Structural and Physical Properties of as-Synthesized Co-Mn Ferrite Nanoparticles by Adding Cr Ions

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Last updated: 23 Jan 2023

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Abstract

In this paper, mixed spinel Co-Mn-Cr ferrite with varying chromium content have been investigated to deduce the relation between the structure and some physical properties; electric, optical and magnetic.
 Nano-crystalline Co0.7Mn0.3CrxFe2-xO4 (x = 0.0, 0.2, 0.4, 0.6, 0.8, and 1) were synthesized via co-precipitation route. The obtained particle size from transmission electron microscope (TEM) micrographs is close to the crystallite size calculated from X-ray diffraction (XRD) by Sherrer's formula, and the particle size distribution is regular. The infrared spectra represent two strong absorption bands around 600 - 400 cm−1, which confirm the presence of M-O stretching bond. The mechanical properties enhanced by adding Cr3+ ions. The optical band-gap calculated from UV-visible spectroscopy is quite affected by adding Cr3+ ions because of particle size reduction. The saturation magnetization (Ms) and the coercivity (Hc) decrease with Cr3+ ions substitution. The variations of the electrical conductivity and drift mobility with temperature were also investigated. The conduction mechanism changed from electron hopping to polaron hopping by raising the temperature. Superparamagnetic Co0.7Mn0.3CrxFe2-xO4 (x ≥ 0.6) nanocrystals can be used in biomedical applications and low power-loss applications. The sample Co0.7Mn0.3Cr0.2Fe1.8O4 has high squareness ratio (Mr/Ms) and, it may be suitable for memory applications.
 

DOI

10.21608/ejs.2020.147994

Volume

42

Article Issue

1

Related Issue

21742

Issue Date

2020-10-01

Receive Date

2019-09-17

Publish Date

2020-10-01

Page Start

1

Page End

20

Print ISSN

1012-5566

Online ISSN

2735-5640

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https://ejs.journals.ekb.eg/article_147994.html

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https://ejs.journals.ekb.eg/service?article_code=147994

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1

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Original Article

Type Code

1,717

Publication Type

Journal

Publication Title

Egyptian Journal of Solids

Publication Link

https://ejs.journals.ekb.eg/

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Article

Created At

23 Jan 2023