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173266

Preparation and Characterization of some Polyalkylarylamines.

Article

Last updated: 22 Jan 2023

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Mathematics and Engineering Physics

Abstract

Adducts of polyalkylarylamines will stoichiometric amounts of stannous chloride were obtained by the reaction of 1,2-dichloroethane with m-phenylenediamine, p-phenylenediamine and 4,4 diaminodiphenyl in the presence of hydrochloric acid and stoichiometric amounts of stannous chloride in methanol as a solvent. Also, adduct of poly (chloromethyne-co- 4,4-dianiinodiphenyl) was obtained from the reaction of chloroform and benzidine by similar method. The structure of these adducts was confirmed by JR spectroscopy, as well 0.X-ray diffractometery, These adducts when reacted with aqueous solution of ammonium carbonate gave the corresponding polyalkylaryl-amine hydrochlorides. Also thermal analysis of these adducts were carried out . 
 

DOI

10.21608/bfemu.2021.173266

Authors

First Name

A.

Last Name

Shaaban

MiddleName

-

Affiliation

Department of Chemistry., Faculty of Science., Zagazig University (Benha Branch)., Benha., Egypt.

Email

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City

-

Orcid

-

First Name

M.

Last Name

El-Komy

MiddleName

A.

Affiliation

Department of Physical and Mathematical Science., Faculty of Engineering (Shoubra)., Zagazig University., (Benno Branch., Cairo., Egypt.

Email

-

City

-

Orcid

-

First Name

A.

Last Name

Al-Sarwy

MiddleName

A.

Affiliation

Department of Physical and Mathematical Science., Faculty of Engineering (Shoubra)., Zagazig University., (Benno Branch., Cairo., Egypt.

Email

-

City

-

Orcid

-

First Name

I.

Last Name

Rashed

MiddleName

Gar Al-Alam

Affiliation

Associate Professor., Department of Physical Science., Faculty of Engineering., Mansoura University., El-Mansoura., Egypt.

Email

-

City

Mansoura

Orcid

-

Volume

13

Article Issue

2

Related Issue

25101

Issue Date

1988-12-01

Receive Date

1988-10-11

Publish Date

2021-05-29

Page Start

27

Page End

37

Print ISSN

1110-0923

Online ISSN

2735-4202

Article File

BFEMU_Volume 13_Issue 2_Pages 27-37.pdf

PDF . 583.5kB

Link

https://bfemu.journals.ekb.eg/article_173266.html

Detail API

https://bfemu.journals.ekb.eg/service?article_code=173266

Order

18

Type

Research Studies

Type Code

1,205

Publication Type

Journal

Publication Title

MEJ. Mansoura Engineering Journal

Publication Link

https://bfemu.journals.ekb.eg/

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Article

Created At

22 Jan 2023