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106800

Synthesis, Characterization of Cu(I) Complex of Thiosemicarbazone Ligand and Antibacterial Activity of Cu(I) Complex.

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Last updated: 22 Jan 2023

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Abstract

Novel complex of Cu(I) of ligand 2-(Anilinoacetyl)-N-phenylhydrazine-1-carbothioamide (H2L) has been synthesized and characterized by 1HNMR, IR, elemental analyses, molar conductance, UVvisible spectra, magnetic susceptibility measurements and thermogravimetric analysis (TGA/DTG). The result confirmed that the ligand behaved as neutral bidentate, coordination take place via carbonyl oxygen(C=O) and N(2)H groups. Copper complex is more thermally stable than free ligand. Copper(I) complexes is mononuclear, adopt octahedral geometry. The ligand and complex have been tested for their inhibitory effect on the growth of bacteria against gram-positive (Streptococcus pyogenes) and gram negative (Escherichia coli). The results proved that the copper complex has less potent antibacterial as compared to the ligand.

DOI

10.21608/rjab.2018.106800

Keywords

complex, IR, Thermal analysis, Antibacterial

Authors

First Name

Nashwa

Last Name

Rizk

MiddleName

M. H.

Affiliation

Department of Environmental Biotechnology, Genetic Engineering and Biotechnology Research Institute, University of Sadat City, Egypt.

Email

nashwa.rizk@gebri.usc.edu.eg

City

-

Orcid

0000-0001-8484-5294

First Name

Samar

Last Name

Aly

MiddleName

A.

Affiliation

Department of Environmental Biotechnology, Genetic Engineering and Biotechnology Research Institute, University of Sadat City, Egypt.

Email

samarchem@yahoo.com

City

-

Orcid

-

First Name

Ayman

Last Name

Eldourghamy

MiddleName

S.

Affiliation

Department of Environmental Biotechnology, Genetic Engineering and Biotechnology Research Institute, University of Sadat City, Egypt.

Email

-

City

-

Orcid

-

First Name

Magda

Last Name

El-Salamony

MiddleName

A.

Affiliation

Clinical pathology Laboratory Department, Students Hospital, University of Sadat City, Egypt.

Email

-

City

-

Orcid

-

First Name

Asmaa

Last Name

Hashad

MiddleName

S.

Affiliation

Department of Environmental Biotechnology, Genetic Engineering and Biotechnology Research Institute, University of Sadat City, Egypt.

Email

-

City

-

Orcid

-

Volume

4

Article Issue

2

Related Issue

16177

Issue Date

2018-11-01

Receive Date

2020-08-09

Publish Date

2018-11-01

Page Start

30

Page End

38

Print ISSN

2356-9433

Online ISSN

2682-3470

Article File

RJAB_Volume 4_Issue 2_Pages 30-38.pdf

PDF . 341.6kB

Link

https://rjab.journals.ekb.eg/article_106800.html

Detail API

https://rjab.journals.ekb.eg/service?article_code=106800

Order

4

Type

Original Article

Type Code

890

Publication Type

Journal

Publication Title

Research Journal of Applied Biotechnology

Publication Link

https://rjab.journals.ekb.eg/

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Article

Created At

22 Jan 2023