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49898

DETERMINATION OF IONS (ANION AND CATION) BY ION CHROMATOGRAPHY IN DRINKING WATER FROM TALKHA TERRITORY AND SOME ITS VILLAGES, DAKAHLIA, EGYPT

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Last updated: 24 Dec 2024

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Abstract

A simple, fast and sensitive ion chromatography (IC) method, for the determination of common inos (anion and cation) in water samples was developed. For comparison, selected samples of tap water, underground water, bottled mineral water and filtered tap water were collected and determined from Talkha and some villages, Dakahlia, Egypt. Ten ions of each anion and cation (fluoride, chloride, bromide, nitrate, sulphate, sodium, ammonium, magnesium, potassium, and calcium) were separated and analyzed, respectively. An isocratic elution with 4.5mmol/L Na2CO3, 1.0 mmol/L NaHCO3 and 42 mmol/L methanesulfonic acid (MSA), IonPac AS22 and CS16 as the separation column and DS6 heated conductivity detector was used. The validation of the analytical method was studied in terms of linearity, sensitivity and accuracy. The linearity was between 0.9922 and 0.9992. And the detection limits ranged from 0.4µg/L to 72µg/L (S/N = 3) and satisfactory repeatability (RSD < 2.82%, n = 6).The recoveries were between 91.3% and 116.6%. All water samples were within the safety and acceptable levels of the World Health Organization (WHO, 2006) guidelines. Out of the samples of drinking water, only underground water had the slightly higher levels. 

DOI

10.21608/jacb.2014.49898

Keywords

Drinking water, Water analysis, Talkha; Egypt, Ion chromatography, anions, cations

Authors

First Name

D.H.

Last Name

Dawood

MiddleName

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Affiliation

Agric. Chem. Dept. Fac. of Agric., Mans. Univ., Mansoura Egypt.

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First Name

M. I.

Last Name

Sanad

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Affiliation

Agric. Chem. Dept. Fac. of Agric., Mans. Univ., Mansoura Egypt.

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Volume

5

Article Issue

9

Related Issue

7720

Issue Date

2014-09-01

Receive Date

2014-09-08

Publish Date

2014-09-01

Page Start

215

Page End

226

Print ISSN

2090-3626

Online ISSN

2090-3707

Link

https://jacb.journals.ekb.eg/article_49898.html

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https://jacb.journals.ekb.eg/service?article_code=49898

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Original Article

Type Code

883

Publication Type

Journal

Publication Title

Journal of Agricultural Chemistry and Biotechnology

Publication Link

https://jacb.journals.ekb.eg/

MainTitle

DETERMINATION OF IONS (ANION AND CATION) BY ION CHROMATOGRAPHY IN DRINKING WATER FROM TALKHA TERRITORY AND SOME ITS VILLAGES, DAKAHLIA, EGYPT

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Article

Created At

22 Jan 2023