Recovery of separated pure concentrates of Cu, REEs, U and V from sulfate leach liquor of southwestern Sinai poly-mineralized ore material was carried out by using different extraction techniques namely; cementation, direct precipitation and ion exchange. These techniques were applied upon the prepared sulfate leach liquor which assaying in g/L: 3.4 Cu, 0.33 REEs, 0.92 U, 0.19 V when using the optimum conditions of H2SO4 acid pug leaching (1.35 ton H2SO4/t ore, at 110C as curing temperature and 2 h as a curing time). A tentative flow sheet for the overall treatment of Abu Zienema poly-mineralized ore material was also presented.