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14704

Synthesis and characterization of Zn(II), Cu(II), Co(II), Ni(II), Cd(II) and Ru(III) ions with a tridentate NNO thiazole derived Schiff base

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Last updated: 24 Dec 2024

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Abstract

Thermal reaction of Co(II), Ni(II), Cu(II), Zn(II), Cd(II) and Ru(III) metal ions with a tridentate Schiff-base ligand(HL) derived from the condensation of 2-aminothiazole and 2-hydroxy-1-naphthaldehyde resulted in the formation of a series of six new metal complexes: [Co(HL)2Cl2]; 1,[Ni(L)(CH3COO)(H2O)]; 2,[Cu(L)2]; 3, [Zn(L)2]; 4, [Cd(L)(CH3COO) (H2O)]H2O; 5, [Ru(L)2(H2O)2]Cl; 6. The ligand and its complexes were characterized by means of elemental and thermal analyses along with molar conductance and magnetic moment measurements as well as different spectroscopic techniques. The ESR spectrum of Cu(II) complex indicated elongated and covalent character of octahedral environment.  

DOI

10.21608/jsrs.2018.14704

Keywords

Spectroscopic studies, Schiff base, Transition metal complexes, Thermal studies

Authors

First Name

Samir

Last Name

El-Medanib

MiddleName

M.

Affiliation

Chemistry Department, Faculty of Science, El-Fayoum University, 63514, El-Fayoum, Egypt.

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First Name

Ayman

Last Name

Abdel Aaziza

MiddleName

A.

Affiliation

Chemistry Department, Faculty of Science, Ain Shams University, 11566, Abbassia, Cairo, Egypt.

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First Name

Rania

Last Name

Mohamed

MiddleName

G.

Affiliation

Chemistry Department, Faculty of Science, El-Fayoum University, 63514, El-Fayoum, Egypt.

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-

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-

Orcid

-

First Name

Abdelmoneim

Last Name

Makhlouf

MiddleName

A.

Affiliation

Chemistry Department, Faculty of Science, El-Fayoum University, 63514, El-Fayoum, Egypt.

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City

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Orcid

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First Name

Sherin

Last Name

Mosad

MiddleName

A.

Affiliation

Chemistry Department, Faculty of Science, El-Fayoum University, 63514, El-Fayoum, Egypt

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Volume

34

Article Issue

part1

Related Issue

2422

Issue Date

2017-09-01

Receive Date

2018-09-25

Publish Date

2017-09-01

Page Start

510

Page End

525

Print ISSN

2356-8364

Online ISSN

2356-8372

Article File

JSRS_Volume 34_Issue part1_Pages 510-525.pdf

PDF . 832.2kB

Link

https://jsrs.journals.ekb.eg/article_14704.html

Detail API

https://jsrs.journals.ekb.eg/service?article_code=14704

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Original Article

Type Code

656

Publication Type

Journal

Publication Title

Journal of Scientific Research in Science

Publication Link

https://jsrs.journals.ekb.eg/

MainTitle

Synthesis and characterization of Zn(II), Cu(II), Co(II), Ni(II), Cd(II) and Ru(III) ions with a tridentate NNO thiazole derived Schiff base

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Article

Created At

22 Jan 2023