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7208

Synthesis of multifunctional acrylate monomers (MFAMs) and their applications

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Last updated: 03 Jan 2025

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-

Tags

Chemistry

Abstract

Novel multifunctional acrylate monomers (MFAMs) were synthesized by reaction of acryloyl chloride with 3,4,5-trihydroxybenzoic (Gallic) acid and diethanolamine in the presence of triethylamine as catalyst. The prepared multifunctional acrylate monomers were used as cross-linkers for the synthesis of polyacrylic acid by precipitation polymerization using 2,2'-azobisisobutyronitrile (AIBN) as free radical initiator. Differential scanning calorimetry studies showed that the glass transition temperature behavior is significantly affected by the type and amount of MFAM employed. Viscosity measurements showed that the thickening effect depend upon the cross-linker type and concentration.

DOI

10.21608/absb.2012.7208

Keywords

Multifunctional acrylate monomers, Gallic acid, diethanolamine, precipitation polymerization, Azobisisobutyro-nitrile, and Differential scanning calorimetry

Authors

First Name

FAHIM

Last Name

NASSAR

MiddleName

-

Affiliation

Department of Applied Chemistry, Faculty of Science, Al-Azhar University, Cairo, Egypt.

Email

-

City

-

Orcid

-

First Name

H.

Last Name

NASSAR

MiddleName

S.

Affiliation

Department of Applied Chemistry, Faculty of Science, Al-Azhar University, Cairo, Egypt.

Email

-

City

-

Orcid

-

First Name

F.

Last Name

HAI

MiddleName

ABDEL

Affiliation

Department of Applied Chemistry, Faculty of Science, Al-Azhar University, Cairo, Egypt.

Email

-

City

-

Orcid

-

First Name

G.

Last Name

AHMED

MiddleName

I.

Affiliation

Department of Applied Chemistry, Faculty of Science, Al-Azhar University, Cairo, Egypt.

Email

-

City

-

Orcid

-

Volume

23

Article Issue

Issue 2-A

Related Issue

1369

Issue Date

2012-12-01

Receive Date

2012-01-01

Publish Date

2012-12-01

Page Start

151

Page End

162

Print ISSN

1110-2535

Online ISSN

2636-3305

Article File

ABSB_Volume 23_Issue Issue 2-A_Pages 151-162.pdf

PDF . 1.3MB

Link

https://absb.journals.ekb.eg/article_7208.html

Detail API

https://absb.journals.ekb.eg/service?article_code=7208

Order

7

Type

Original Article

Type Code

520

Publication Type

Journal

Publication Title

Al-Azhar Bulletin of Science

Publication Link

https://absb.journals.ekb.eg/

MainTitle

Synthesis of multifunctional acrylate monomers (MFAMs) and their applications

Details

Type

Article

Created At

22 Jan 2023