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7097

APPLICATION OF 23 FULL-FACTORIAL DESIGN FOR DEVELOPMENT AND OPTIMIZATION OF BIOCOMPATIBLE, BIODEGRADABLE SOLID LIPID NANOPARTICLES CONTAINING CURCUMIN

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Last updated: 22 Jan 2023

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Abstract

Curcumin (C), a natural anticancer agent suffers extremely low aqueous solubility and rapid systemic elimination, therefore,  the aim from the present study was to develop and optimize biocompatible, biodegradable solid lipid nanoparticles containing curcumin (CSLNs) using Solvent Injection Method. The components selected to develop the SLNs were Glycerol MonoStearate (GMS; the lipidic carrier), Poloxamer 407 (P407; Surfactant) and Ethanol (solvent for the drug and the lipidic carrier). The combination and ratios for the optimization process were carried out using 23 full-factorial designs. The experimental design runs (8 formulations H1–H8) were prepared and the design dependent responses (assessment of particle size, Entrapment Efficiency % and the in vitro release study) were characterized. The developed formulae showed a nanometric particle size range (203.0–345.0nm), high Entrapment Efficiency % (62.77–87.42 %) and prolonged release over 24 hr periods (55.97–89.64 %). These results were analyzed using JMP® 10 software and its analytical tools were used to draw Pareto charts and the interactions plots. On the basis of the software analysis, formulation H9 with a desirability factor of 0.582 was selected as the optimized formulation and was evaluated for the dependent responses. Formulation H9 showed a particle size of 249.1 nm, 74.51 % Entrapment efficiency, 85.72 % in vitro release over 24 hr and these results suggested that the solid lipid nanoparticles formulations could be a promising method to sustain the release of curcumin.

DOI

10.21608/ajps.2013.7097

Authors

First Name

Hamdy

Last Name

Dawaba

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Affiliation

Department of Pharmaceutics and Industrial Pharmacy, College of Pharmacy, Al-Azhar University – Cairo, Egypt.

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Volume

48

Article Issue

2

Related Issue

1338

Issue Date

2013-09-01

Receive Date

2018-05-14

Publish Date

2013-09-01

Page Start

84

Page End

101

Print ISSN

1110-1644

Online ISSN

2535-1958

Link

https://ajps.journals.ekb.eg/article_7097.html

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https://ajps.journals.ekb.eg/service?article_code=7097

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6

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Original Article

Type Code

518

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Journal

Publication Title

Al-Azhar Journal of Pharmaceutical Sciences

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https://ajps.journals.ekb.eg/

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Article

Created At

22 Jan 2023