145825

DETERMINATION OF SOME ESSENTIAL AND TOXIC ELEMENTS OF COMMERCIAL CHILDREN FOOD IN THE EGYPTIAN MARKETS

Article

Last updated: 03 Jan 2025

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Tags

Agriculture

Abstract

The present work was carried out for determination of Antimony (Sb), cadmium (Cd), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), Manganese (Mn), nickel (Ni), Tin (Sn) and zinc (Zn) in children food samples using inductively coupled plasma optical emission spectrometer (ICP-OES). The method showed that the quantification limits were varied between 0.02 and 1 mg/kg. The mean recoveries ± standard deviations at different spiking levels were varied between 81.95 ± 3.89 and 112.56 ± 3.31 % with coefficient of variation expressed as relative standard deviation ranged from 1.95 and 5.91%. The method trueness was confirmed by using three different certified references materials purchased from (WEPAL) and all obtained results were with in satisfactory ranges and had acceptable recovery and Z-score values. The method precision, in terms of relative standard deviation (RSD), was being below 5.16 % .The method uncertainty expressed as expanded uncertainty of all validated elements was found to be ≤ 22.68 %. The results obtained make the method suitable for accurate determination of validated elements in different kinds of children food samples at these low concentration values. Validated method was used for the determination of metallic contaminants in 50 samples covering 19 different brands of popular biscuits, snacks, cooked potato, bake, and cake in Egypt. The result showed that, all tested samples were free from any detectable amount of Pb. On the other hand, the resulting concentration ranges, in mg/kg, were as follows: < 0.02–0.08 (Cd), < 1– 10.9 (Cu), 3.4 – 227.1 (Fe), 1.2 – 7.6 (Mn), 1.2 – 3.8 (Ni), 1 – 3.5 (Sn), and 3 – 269.1 (Zn).
 

DOI

10.21608/jes.2019.145825

Keywords

Keywords: Children food, ICP-OES, Essential and toxic elements, Egypt

Authors

First Name

Maha A.

Last Name

Souror

MiddleName

-

Affiliation

Ministry of Agriculture and Land Reclamation, Agricultural Research Center, Central Laboratory of Residue Analysis of Pesticides and Heavy Metals in Foods (QCAP Egypt),

Email

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City

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Orcid

-

First Name

Mohammed I.

Last Name

Abdel Megeed

MiddleName

-

Affiliation

Plant Protection Department, Faculty of Agriculture, Ain Shams University

Email

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City

-

Orcid

-

First Name

And Mona A.

Last Name

Khorshed

MiddleName

-

Affiliation

Plant Protection Department, Faculty of Agriculture, Ain Shams University

Email

-

City

-

Orcid

-

Volume

48

Article Issue

2

Related Issue

21423

Issue Date

2019-12-01

Receive Date

2019-12-02

Publish Date

2019-12-01

Page Start

87

Page End

113

Print ISSN

1110-0826

Online ISSN

2636-3178

Link

https://jes.journals.ekb.eg/article_145825.html

Detail API

https://jes.journals.ekb.eg/service?article_code=145825

Order

5

Type

Review Article

Type Code

599

Publication Type

Journal

Publication Title

Journal of Environmental Science

Publication Link

https://jes.journals.ekb.eg/

MainTitle

DETERMINATION OF SOME ESSENTIAL AND TOXIC ELEMENTS OF COMMERCIAL CHILDREN FOOD IN THE EGYPTIAN MARKETS

Details

Type

Article

Created At

22 Jan 2023