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62247

Preparation and Characterization of TiO2-SiO2 Bioceramic Coating on Ti Alloy via Electrochemical Anodization and Its Effect on Corrosion Resistance

Article

Last updated: 22 Jan 2023

Subjects

-

Tags

Dental Biomaterials

Abstract

Abstract
Purpose: The present study was carried out to study changing the anodization parameters and investigate the corrosion resistance of the ceramic coating that will be formed on the CP-Ti by anodization method. Materials and Methods: CP-Ti (10mm×10mm×2mm) were used for fabrication of bioceramic coating through anodization with different parameters using potassium silicate electrolyte. Samples were characterized using XRD, AT-FTIR. Surface roughness was measured using ESEM and surface topography was evaluated by SEM. Tafel polarization and electrochemical impedance spectroscopy were used to detect the change in the corrosion resistance after anodization. Results: XRD revealed that the anodized coated samples showed well defined peaks of Ti and TiO2 and shallow peaks of SiO2. AT-FTIR showed stretching bands of titania and silica. Surface roughness results: anodized coated samples at the optimum conditions had the lowest Ra values while the uncoated group had the highest Ra value. Results of the surface morphology: best evenly distributed ceramic coat was formed at the optimum conditions where (the applied voltage =50v, the electrolyte concentration =3% and process duration=60min). Corrosion resistance of the anodized coated samples at the optimum conditions was markedly increased more than that of the uncoated CP-Ti. Conclusions:optimum conditions of the anodization process to get a uniform anodized coating can be achieved when; the applied voltage is 50v, the electrolyte concentration is 3% and the process duration in 60min. Moreover, formation of a bioceramic coating has been shown to be a useful method for improving the corrosion resistance.

DOI

10.21608/adjg.2019.6218.1058

Keywords

Anodization, CP-Ti implant, Corrosion Resistance, Surface Morphology

Authors

First Name

rasha

Last Name

marzouk

MiddleName

mohammed

Affiliation

Associate Lecturer of dental biomaterial,faculty of dental medicine,al-azhar university for girls,cairo, egypt

Email

rashamarzouk@hotmail.com

City

-

Orcid

-

First Name

Eatemad

Last Name

Shoreibah

MiddleName

-

Affiliation

professor of oral medicine and periodontology

Email

eshoreibah@yahoo.com

City

Cairo

Orcid

-

First Name

Inas

Last Name

motawae

MiddleName

talaat

Affiliation

Professor of Dental Biomaterials, Faculty of Dentistry-Girls branch,Alazhar University

Email

inas_72talaat@yahoo.com

City

Cairo

Orcid

-

First Name

madiha

Last Name

shoeib

MiddleName

ahmed

Affiliation

Professor and Former Head of Surface Treatment and Corrosion Control, The Central Metallurgical RD Institute, cairo,egypt

Email

mshoeib@yahoo.com

City

-

Orcid

-

Volume

6

Article Issue

3

Related Issue

6305

Issue Date

2019-07-01

Receive Date

2018-11-14

Publish Date

2019-07-01

Page Start

317

Page End

328

Print ISSN

2537-0308

Online ISSN

2537-0316

Link

https://adjg.journals.ekb.eg/article_62247.html

Detail API

https://adjg.journals.ekb.eg/service?article_code=62247

Order

24

Type

Original Article

Type Code

488

Publication Type

Journal

Publication Title

Al-Azhar Dental Journal for Girls

Publication Link

https://adjg.journals.ekb.eg/

MainTitle

-

Details

Type

Article

Created At

22 Jan 2023