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204786

Green Synthesis by Zygophyllum Coccineum Leaves Extract for Preparing ZnO Nanoparticles, and Characteristics Study.

Article

Last updated: 01 Jan 2025

Subjects

-

Tags

Physical chemistry

Abstract

Abstract
In this paper, we used the aqueous extract of the Zygophyllum Coccineum Plant Leaves for the synthesis of ZnO-NPs by a green method utilizing zinc acetate dihydrate as a precursor. The synthesized zinc oxide NPs was characterized by AFM (Atomic Force Microscopy), UV-Vis. (UV-Visible spectroscopy), FT-IR (Fourier Transform Infrared Spectroscopy). XRD (X-Ray Diffraction), FE-SEM (Field emission Scanning Electron Microscopy), and EDX (Energy Dispersive X-Ray Spectroscopy). We investigate the topography of the ZnO-NPs surface and it gave an average diameter of 67.42 nm. The wavelength of the sample was 368 nm and Eg was 3.3714 e. V. The absorption peak appears at 561 cm-1 which confirms the presence of ZnO-NPs nanoparticles. X-ray diffraction studies represent the size of crystallites 12.01 nm using the Debby-Scherrer formula that proposed ZnO-NPs have a hexagonal structure. The purity of zinc oxide NPs formation and the percentage of elements in nanoparticles structure were proven by EDX. SEM testing using the images of the ZnO-NPs proved that spherical shapes of nanoparticles agree with XRD analysis.

DOI

10.21608/ejchem.2021.102312.4746

Keywords

Zygophyllum Coccineum, Zinc Oxide Nanoparticles, Green method, Biosynthesis, flavonoid

Authors

First Name

Ahmed Magtouf

Last Name

Al-Wadi

MiddleName

-

Affiliation

Department of chemistry, College of science, University of Baghdad, Baghdad, Iraq.  

Email

amwiraq@yahoo.com

City

Baghdad

Orcid

0000-0001-8584-0233

First Name

Dunya Edan

Last Name

Al-Mammar

MiddleName

-

Affiliation

Department of chemistry, College of science, University of Baghdad, Baghdad, Iraq.  

Email

-

City

-

Orcid

-

Volume

65

Article Issue

5

Related Issue

29749

Issue Date

2022-05-01

Receive Date

2021-10-22

Publish Date

2022-05-01

Page Start

363

Page End

369

Print ISSN

0449-2285

Online ISSN

2357-0245

Link

https://ejchem.journals.ekb.eg/article_204786.html

Detail API

https://ejchem.journals.ekb.eg/service?article_code=204786

Order

36

Type

Original Article

Type Code

297

Publication Type

Journal

Publication Title

Egyptian Journal of Chemistry

Publication Link

https://ejchem.journals.ekb.eg/

MainTitle

Green Synthesis by Zygophyllum Coccineum Leaves Extract for Preparing ZnO Nanoparticles, and Characteristics Study.

Details

Type

Article

Created At

22 Jan 2023