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178848

DISSIPATION OF CYFLUMETOFEN IN STRAWBERRY FRUITS AND GREEN BEAN PODS UNDER GREENHOUSE CONDITIONS USING QUECHERS METHOD AND GC/(μ-ECD)

Article

Last updated: 01 Jan 2025

Subjects

-

Tags

Environmental chemistry

Abstract

Strawberry and green bean are important cash crops. Both are highly infected by different pests under greenhouse conditions causing reduction in quality and yield. Mites are usually from the most common pests of beans and strawberries. Field experiment was carried out to investigate dissipation of Cyflumetofen (a novel acaricide) in strawberry fruits and green bean pods. Determination was done using quick, easy, cheap, effective, rugged, safe (QuEChERS) method and cleanup step utilizing dispersive solid-phase extraction (DSPE) followed by gas chromatography coupled with a micro electron capture detector GC/(μ-ECD). Average recoveries were within 80.75-92.15% and 80.86-82.91%, with relative standard deviations (RSDs) ranging from 2.8 to 6.6% and 3.59-4.70%. in strawberry and green bean samples, respectively at spiking levels (0.01 - 1 mg/kg). Linearity was achieved for Cyflumetofen with correlation coefficient R2 > 0.98 and matrix-matched calibration also showed linearity with determination coefficients R2 > 0.98. The initial deposits in strawberry fruits and green bean pods were 2.48 and 3.24 mg/kg, respectively. The half-life period (RL50) in strawberry fruits and green bean pods was 1.81 and 1.16 days, respectively. According to maximum residue level (MRL) which is 0.6 mg/kg, the pre-harvest interval (PHI) was estimated to be 3 days in strawberry fruits.

DOI

10.21608/ejchem.2021.77606.3787

Keywords

Cyflumetofen, GC-(μ-ECD), Dissipation, QuEChERS, strawberry, green bean

Authors

First Name

El Desoky

Last Name

Ibrahim

MiddleName

-

Affiliation

Department of Economic Entomology and Pesticides, Faculty of Agriculture Cairo University

Email

aldosokyibrahim@yahoo.com

City

-

Orcid

0000-0003-0109-630X

First Name

Dalia

Last Name

El-Hefny

MiddleName

-

Affiliation

Pesticides Residues and Environmental Pollution Dept., Central Agricultural Pesticides Laboratory, Agricultural Research Center, Giza, Egypt.

Email

-

City

-

Orcid

-

Volume

64

Article Issue

11

Related Issue

27064

Issue Date

2021-11-01

Receive Date

2021-05-25

Publish Date

2021-11-01

Page Start

6,799

Page End

6,807

Print ISSN

0449-2285

Online ISSN

2357-0245

Link

https://ejchem.journals.ekb.eg/article_178848.html

Detail API

https://ejchem.journals.ekb.eg/service?article_code=178848

Order

63

Type

Original Article

Type Code

297

Publication Type

Journal

Publication Title

Egyptian Journal of Chemistry

Publication Link

https://ejchem.journals.ekb.eg/

MainTitle

DISSIPATION OF CYFLUMETOFEN IN STRAWBERRY FRUITS AND GREEN BEAN PODS UNDER GREENHOUSE CONDITIONS USING QUECHERS METHOD AND GC/(μ-ECD)

Details

Type

Article

Created At

22 Jan 2023