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156878

Synthesis, Characterization, scaling up and use of Calcium Carbonate Nanoparticles to prepare nanoporous PVC film

Article

Last updated: 22 Jan 2023

OverviewSimilar Items

Subjects

-

Tags

Nano chemistry

Abstract

CaCO3 nanoparticles were synthesized from CaCl2 and Na2CO3 using a new, fast and straightforward technique. Factors affecting on the particle size such as the concentration of Ca2+ and CO32-, PEG weight dissolved in Ca2+ solution, flow rate, temperature, media type, PEG weight dissolved in the used medium, the concentration of CO32-, stirring speed, medium volume and additive dissolved within Ca2+ solution were investigated. The obtained particles were characterized by SEM, XRD, EDS, IR and TGA. The characterization clarified that the particles prepared were spherical with a size range of 19-30 nm, ultra-pure, and calcite. Moreover, the preparation system was redesigned to be a continuous preparation system. The histogram showed that the CaCO3 nanoparticles obtained were homogenous in size (30 nm). Finally, the obtained nanoparticles were utilized in the preparation of nanoporous PVC film with pores size range 80-120nm

DOI

10.21608/ejchem.2021.49234.3012

Keywords

Keywords:CaCO3 nanoparticles, calcite, precipitation, chemical control reaction, spherical, nanopores film

Authors

First Name

Ahamed

Last Name

Abd-Elhamid

MiddleName

I

Affiliation

Universities and Research Centres District

Email

ahm_ch_ibr@yahoo.com

City

Alexandria

Orcid

-

First Name

H.

Last Name

Aly

MiddleName

F.

Affiliation

Hot Laboratories Centre, Atomic Energy Authority,13759, Egypt

Email

maysamohamed19@yahoo.com

City

Cairo

Orcid

-

First Name

Hesham

Last Name

Soliman

MiddleName

M.A.

Affiliation

Advanced Technology and New Materials Research Institute, City of Scientific Research and Technology Applications, P. O. Box 21934, Alexandria, Egypt

Email

h.soliman@srtacity.sci.eg

City

Alexandria

Orcid

0000-0003-4000-1297

First Name

M.

Last Name

Akl

MiddleName

A.

Affiliation

Faculty of Science, Mansoura University.

Email

ttamer85@yahoo.com

City

Mansoura

Orcid

-

First Name

Aref

Last Name

Abd ELRahman

MiddleName

M.E

Affiliation

nanotechnology depaetment

Email

drareff@gmail.com

City

Alexandria

Orcid

-

First Name

tamer

Last Name

elrazik

MiddleName

abd

Affiliation

City of Scientific Research and technological applications (SRTA)

Email

ttamer85@gmail.com

City

New Borg Elarab

Orcid

0000-0002-6203-7488

Volume

64

Article Issue

7

Related Issue

25275

Issue Date

2021-07-01

Receive Date

2020-11-14

Publish Date

2021-07-01

Page Start

3,623

Page End

3,634

Print ISSN

0449-2285

Online ISSN

2357-0245

Article File

EJCHEM_Volume 64_Issue 7_Pages 3623-3634.pdf

PDF . 5.5MB

Link

https://ejchem.journals.ekb.eg/article_156878.html

Detail API

https://ejchem.journals.ekb.eg/service?article_code=156878

Order

39

Type

Original Article

Type Code

297

Publication Type

Journal

Publication Title

Egyptian Journal of Chemistry

Publication Link

https://ejchem.journals.ekb.eg/

MainTitle

-

Details

Type

Article

Created At

22 Jan 2023