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156884

Synthesis and Characterization of some Tetrazole Derivatives and Evaluation of their Biological Activity

Article

Last updated: 22 Jan 2023

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Tags

Organic chemistry

Abstract

This research included synthesizing a series of heterocyclic compounds where the compound 2-chloroacetohydrazide was synthesized from ethyl chloroethanoate with Hydrazine hydrate 95%. The reaction was carried out in the cold condition. 2-(pyrimidin-2-ylamino)acetohydrazide was prepared by reaction A1 with 2-amino pyrimidine in absolute ethanol using Potassium hydroxide (KOH); then reaction 2-(pyrimidin-2-ylamino) acetohydrazide with different aldehydes to produce Schiff bases derivatives A3 –A14 which was introduced in two different synthetic methods the first was synthesized. Then tetrazole derivatives [A15-A19] were synthesized from the hydrozone reactor (Schiff bases) [A3-A14] prepared by reaction Schiff base with sodium azide. In a second way, derivatives 2, 3-dihydroquinozoline-4-one [A20-A24] were synthesized from the interaction of some of Schiff's bases in the third step with anthralenic acid (2-amino benzoic acid) using 1,4-dioxane as a solvent; the synthetic compounds were diagnosed with some spectral methods, such as UV, FTIR, 1H-NMR and quantitative analysis of the elements (C.H.N.S.). Some synthetic compounds on the growth of four types of bacterial isolates known to be resistant to antibiotics were studied. Amoxicillin and Ampicillin were used as control samples, and some of the prepared compounds showed good inhibiting efficacy against the used bacteria (Escherichia coli, Klebsiella pneumonia, Staphylococcus aureus, and Staphylococcus epidermidis)

DOI

10.21608/ejchem.2021.54356.3165

Keywords

Heterocyclic compounds, ring-closing reaction, Tetrazole, 2-amino pyrimidine

Authors

First Name

Sanaa A.

Last Name

Alsahib

MiddleName

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Affiliation

Department of Chemistry, College of Science for Women University of Baghdad

Email

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City

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Orcid

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First Name

Ruaa M.

Last Name

Dhedan

MiddleName

-

Affiliation

Department of Chemistry, College of Science for Women University of Baghdad

Email

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City

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Orcid

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Volume

64

Article Issue

6

Related Issue

24623

Issue Date

2021-06-01

Receive Date

2020-12-26

Publish Date

2021-06-01

Page Start

2,925

Page End

2,936

Print ISSN

0449-2285

Online ISSN

2357-0245

Link

https://ejchem.journals.ekb.eg/article_156884.html

Detail API

https://ejchem.journals.ekb.eg/service?article_code=156884

Order

21

Type

Original Article

Type Code

297

Publication Type

Journal

Publication Title

Egyptian Journal of Chemistry

Publication Link

https://ejchem.journals.ekb.eg/

MainTitle

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Details

Type

Article

Created At

22 Jan 2023