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82067

A Novel Method for The Preparation of Conductive Methyl Cellulose-Silver Nanoparticles-Polyaniline-Nanocomposite

Article

Last updated: 01 Jan 2025

Subjects

-

Tags

Textile chemistry

Abstract

A novel green method for the synthesis of conductive nanocomposite -using silver nitrate, methyl cellulose (MC), glycerol, and aniline- was adopted. Here, silver nitrate was used as a precursor, methyl cellulose as both reducing and capping agent, glycerol as a co-reducing and ductility agent and water as solvent. While silver nitrate oxidizes aniline to polyaniline, it is reduced to silver nanoparticles. Doing so, both conductive polyaniline and conductive silver nanoparticle were in-situ synthesized via the formation of methyl cellulose- silver-polyaniline nanocomposite. Reproducibility of the nanocomposite revealed that the synthesis process is consistent. The nanocomposite film was characterized by FTIR, SEM, EDAX, XRD, and conductivity. XRD pattern showed poly crystallinity. TEM of the colloidal solution showed different particle shapes of AgNPs with size from 4-36 nm and d-spacing of 0.22 nm. SAED exhibits ring pattern with bright spots displaying polycrystallinity. Nanocomposite film, coated glass, cotton and polyester fabrics showed promising conductivity.

DOI

10.21608/ejchem.2020.27264.2568

Keywords

Silver nanoparticles, Polyaniline, glycerol, Methyl Cellulose, polycrysallininty, d spacing

Authors

First Name

Manal

Last Name

El-Sheikh

MiddleName

A.

Affiliation

Pre-Treatment and Finishing of Cellulosic Fibres, Textile Research Division, National Research Centre, Egypt

Email

dr.manal.elsheikh@gmail.com

City

Dokki

Orcid

0000-0001-5148-5755

First Name

Amal

Last Name

Al-Enezy

MiddleName

-

Affiliation

Jouf University

Email

amul20030@gmail.com

City

-

Orcid

-

First Name

Fatema

Last Name

El-Enezy

MiddleName

-

Affiliation

Jouf University

Email

fzja33@outlook.sa

City

-

Orcid

-

First Name

Dalil

Last Name

Ashammri

MiddleName

-

Affiliation

Jouf University

Email

ashammri2003@gmail.com

City

-

Orcid

-

First Name

Fatema

Last Name

El-Enezy

MiddleName

-

Affiliation

Jouf University

Email

fatmah_mn@icloud.com

City

-

Orcid

-

First Name

Waad

Last Name

Alrowili

MiddleName

-

Affiliation

Jouf University

Email

waadalrowili@gmail.com

City

-

Orcid

-

Volume

63

Article Issue

9

Related Issue

16781

Issue Date

2020-09-01

Receive Date

2020-04-04

Publish Date

2020-09-01

Page Start

3,567

Page End

3,582

Print ISSN

0449-2285

Online ISSN

2357-0245

Link

https://ejchem.journals.ekb.eg/article_82067.html

Detail API

https://ejchem.journals.ekb.eg/service?article_code=82067

Order

32

Type

Original Article

Type Code

297

Publication Type

Journal

Publication Title

Egyptian Journal of Chemistry

Publication Link

https://ejchem.journals.ekb.eg/

MainTitle

A Novel Method for The Preparation of Conductive Methyl Cellulose-Silver Nanoparticles-Polyaniline-Nanocomposite

Details

Type

Article

Created At

22 Jan 2023