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1393

Synthesis and Reactions of 2-(N-tetrabromophthalimido) Ethyl Acrylate Polymer with Hydroxy and Amino Compounds

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Last updated: 22 Jan 2023

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Abstract

 N-(2-HYDROXYETHYL)tetrabromophthalimide (HETP) was ……prepared by heating tetrabromophthalic anhydride dissolved in dimethyl formamide (DMF) with ethanol amine. 2- (N-tetrabromophthalimido) ethyl acrylate (TPEA) was prepared by the reaction of acryloyl chloride (AC) with N-(2-hydroxyethyl) tetrabromophthalimide (HETP) in presence of triethyl amine(TEA). The resulting monomer was polymerized. The exchange reactions were carried out in solution at 60ºC The structure of prepared polymers and copolymers was investigated by bromine analysis, IR and 1HNMR spectroscopy.

DOI

10.21608/ejchem.2011.1393

Keywords

N- (2- Hydroxyethyl ) tetrabromophthalimide, 2- ( N-tetrabromophthalimido) ethyl acrylate, Acryloyl chloride, Exchange reactions and Copolymers

Volume

54

Article Issue

2

Related Issue

304

Issue Date

2012-04-01

Receive Date

2011-08-01

Publish Date

2011-04-30

Page Start

271

Page End

279

Print ISSN

0449-2285

Online ISSN

2357-0245

Link

https://ejchem.journals.ekb.eg/article_1393.html

Detail API

https://ejchem.journals.ekb.eg/service?article_code=1393

Order

8

Type Code

292

Publication Type

Journal

Publication Title

Egyptian Journal of Chemistry

Publication Link

https://ejchem.journals.ekb.eg/

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Article

Created At

22 Jan 2023