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Development and Crystallization Study of Li2O-B2O3-SiO2 Glass Ceramic Rich with ZrO2

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Last updated: 22 Jan 2023

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Abstract

 GLASS ceramic in the system Li2O-B2O3-SiO2 was prepared by adding different amounts of ZrO2 up to maximum saturation. DTA, XRD and SEM were used to study the crystallization behavior of these glass samples. Tetragonal and monoclinic zirconia, are the only crystallized phases obtained after different heat treatment schedules. Fraction of transformed ZrO2 and total intensity of ZrO2 were calculated. Microhardness was measured for different samples, and it was found to be depending on the amount of ZrO2 added and the heat treatment parameters. Sample contains 20 g ZrO2 and treated at 650ºC for 10 hr showed higher microhardness value (14.99GPa).

DOI

10.21608/ejchem.2011.1381

Keywords

hardness, Glass-ceramic, Borosilicate, Zirconia and Martensitic transformation

Volume

54

Article Issue

1

Related Issue

303

Issue Date

2012-02-01

Receive Date

2011-01-04

Publish Date

2011-02-28

Page Start

81

Page End

97

Print ISSN

0449-2285

Online ISSN

2357-0245

Link

https://ejchem.journals.ekb.eg/article_1381.html

Detail API

https://ejchem.journals.ekb.eg/service?article_code=1381

Order

6

Type Code

292

Publication Type

Journal

Publication Title

Egyptian Journal of Chemistry

Publication Link

https://ejchem.journals.ekb.eg/

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Article

Created At

22 Jan 2023